Termikus folyamattechnika

Cold-Wall Retort Furnaces up to 2400 °C

Retort furnace VHT 500/22-GR H2 with CFC-process box and extension package for operation under hydrogen

Graphite heating chamber

Molybdenum or tungsten heating chamber

Molybdenumdisilicide heater and fiber insulation

The compact retort furnaces of the VHT product line are available as electrically heated chamber furnaces with graphite, molybdenum, tungsten or MoSi2 heating. A wide variety of heating designs as well as a complete range of accessories provide for optimal retort furnace configurations even for sophisticated applications.

The vacuum-tight retort allows heat treatment processes either in protective and reaction gas atmospheres or in a vacuum, subject to the individual furnace specs to 10-5 mbar. The basic furnace is suited for operation with non-flammable protective or reactive gases or under vacuum. The H2 version provides for operation under hydrogen or other flammable gases. Key of the specification up is a certified safety package providing for a safe operation at all times and triggers an appropriate emergency program in case of failure.

Alternative Heating Specifications

In general the following variants are available with respect to the process requirements:

VHT ../..-GR with Graphite Insulation and Heating

  • Suitable for processes under protective and reaction gases or under vacuum
  • Tmax 1800  °C, 2200  °C or 2400 °C (VHT 40/.. - VHT 100/..)
  • Max. vacuum up to 10-4 mbar depending on pump type used
  • Graphite felt insulation

VHT ../..-MO or VHT ../..-W with Molybdenum or Tungsten Heating

  • Suitable for high-purity processes under protective and reaction gases or under high vacuum
  • Tmax 1200  °C, 1600  °C or 1800  °C (see table)
  • Max. vacuum up to 10-5 mbar depending on pump type used
  • Insulation made of molybdenum rsp. tungsten radiation sheets

VHT ../..-KE with Fiber Insulation and Heating through Molybdenum Disilicide Heating Elements

  • Suitable for processes under protective and reaction gases, in air or under vacuum
  • Tmax 1800  °C
  • Max. vacuum up to 10-2 mbar (up to 1300  °C) depending on pump type
  • Insulation made of high purity aluminum oxide fiber
 

Schematic presentation of a cold-wall retort furnace with additional equipment 1 Retort 2 Heating 3 Insulation 4 Gas management system 5 Vacuum pump 6 Cooling water distribution 7 Controls 8 Integrated switchgear 9 Heating transformer 10 Charging frame inside the inner process chamber Retort furnace VHT 8/16MO with automation package

Retort furnace VHT 100/16MO with automation package

Basic version

  • Standard furnace sizes 8 - 500 liters
  • Water-cooled retort made of stainless steel
  • Frame made of stable steel profiles, easy to service due to easily removable stainless steel panels
  • Housing of the VHT 8 model on castors for easy repositioning of furnace
  • Cooling water manifold with manual tap, automatic flow monitoring, open-loop cooling water system
  • Adjustable cooling water circuits with flowmeter and temperature indicator and overtemperature protection
  • Switchgear and controller integrated in furnace housing
  • Process control with controller P470
  • Over-temperature limiter with adjustable cutout temperature for thermal protection class 2 in accordance with EN 60519-2
  • Manual operation of the process gas and vacuum functions
  • Manual gas supply for one process gas (N2, Ar or non-flammable forming gas) with adjustable flow
  • Bypass with manual valve for rapid filling or flooding of furnace chamber
  • Manual gas outlet with overflow valve (20 mbar relative) for over-pressure operation
  • Single-stage rotary vane pump with ball valve for pre-evacuating and heat treatment in a rough vacuum to 5 mbar
  • Pressure gauge for visual pressure monitoring
  • Defined application within the constraints of the operating instructions
 

Retort furnace VHT 40/22-GR with motor-driven lift door and front frame for connection to a glovebox

Heat treatment of copper bars under hydrogen in retort furnace VHT 8/16-MO

Thermocouple, type S with automatic pull-out device for precise control results in the low temperature range

Turbo-molecular pump

Additional equipment housing/heater

  • Housing, optionally divisible, for passing through narrow door frames (VHT 8)
  • Lift door
  • Individual heating concepts

Additional equipment gas management system

  • Manual gas supply for second process gas (N2, Ar or non-flammable forming gas) with adjustable flow and bypass
  • Mass flow controller for alternating volume flow and generation of gas mixtures with second process gas (only with automation package)
  • Inner process box made of molybdenum, tungsten, graphite or CFC, especially recommended for debinding processes. The box is installed in the furnace with direct gas inlet and outlet and provides for better temperature uniformity. Generated exhaust gases will be directly lead out the inner process chamber during debinding. The change of gas inlet pathes after debinding results in a clean process gas atmosphere during sintering.

Additional equipment vacuum

  • Two-stage rotary vane pump with ball valve for pre-evacuating and heat-treating in a fine vacuum (up to 10-2 mbar) incl. electronic pressure sensor
  • Turbo molecular pump with slide valve for pre-evacuation and for heat treatment in a high vacuum (up to 10-5 mbar) including electronic pressure sensor and booster pump
  • Other vacuum pumps on request
  • Partial pressure operation: protective gas flushing at controlled underpressure (only with automation package)

Additional equipment cooling

  • Heat exchanger with closed-loop cooling water circuit
  • Direct cooling

Additional equipment for controls and documentation

  • Charge thermocouple with display
  • Temperature measurement at 2200  °C models with pyrometer in the upper temperature range and thermocouple, type C with automatic pull-out device for precise control results in the low temperature range (VHT 40/..-GR and larger)
  • Automation package with process control H3700
    • 12“ graphic touch panel
    • Input of all process data like temperatures, heating rates, gas injection, vacuum at the touch panel
    • Display of all process-relevant data on a process control diagram
    • Automatic gas supply for one process gas (N2, argon or non-flammable forming gas) with adjustable flow
    • Bypass for flooding and filling the chamber with process gas controlled by the program
    • Automatic pre- and post programs, including leak test for safe furnace operation
    • Automatic gas outlet with bellows valve and overflow valve (20 mbar relative) for over-pressure operation
    • Transducer for absolute and relative pressure
  • Process control and documentation via VCD software package or Nabertherm Control Center (NCC) for monitoring, documentation and control
 

Single-stage rotary vane pump for heat treatment in a rough vacuum to 5 mbar Two-stage rotary vane pump for heat treatment in a vacuum to 10-2 mbar

Graphite inner process chamber incl. charge holder

Molybdenum inner process chamber incl. six charge supports

Process Box for Debinding in Inert Gas

Certain processes require charges to be debinded in non-flammable protective or reactive gases. For these processes we fundamentally recommend a hot-wall retort furnace (see models NR .. or SR ..). These retort furnaces can ensure that the formation of condensation will be avoided as throughly as possible.

If there is no way to avoid the escape of small amounts of residual binder during the process, even in the VHT furnace, the retort furnace should be designed to meet this contingency.

The furnace chamber is equipped with an additional process box that has a direct outlet to the exhaust gas torch through which the exhaust gas can be directly vented. This system enables a substantial reduction in the amount of furnace chamber contamination caused by the exhaust gases generated during debinding.

Depending on the exhaust gas composition the exhaust gas line can be designed to include various options.

  • Exhaust gas torch for burning off the exhaust gas
  • Condensation trap for separating out binding agents
  • Exhaust gas post-treatment, depending on the process, via scrubbers
  • Heated exhaust gas outlet to avoid condensation deposits in the exhaust gas line
 VHT ../..-GRVHT ../..-MOVHT ../18-WVHT ../18-KE
Tmax1800 °C, 2200 °C or 2400 °C1200 °C or 1600 °C1800 °C1800 °C
Inert gas
Air/Oxygen---
Hydrogen3,4331,3
Rough vacuum and fine vacuum (>10-3 mbar)2
High vacuum (<10-3 mbar)42
Material of heaterGraphiteMolybdenumTungstenMoSi2
Material of insulationGraphite feltMolybdenumTungsten/MolybdenumCeramic fiber
1Tmax reduces to 1400 °C 3Only with safety package for flammable gases 2Depending on the temperature 4Up to 1800 °C
ModelInner dimensions of process box in mmVolume
 wdhin l
VHT 8/..1202101503,5
VHT 25/..20035020014,0
VHT 40/..25043025025,0
VHT 70/..32547532550,0
VHT 100/..42550042590,0
VHT 250/..575700575230,0
VHT 500/..725850725445,0
ModelInner dimensions in mmVolumeMax. chargeOuter dimensions in mmHeating power in kW4
 wdhin lweight/kgWDHGraphiteMolybdenumTungstenCeramic fiber
VHT 8/..170240200851250 (800)111002700527/27/-219/3435012
VHT 25/..250400250252015002500220070/90/-245/6538525
VHT 40/..3004503004030160026005230083/103/125254/90311030
VHT 70/..375500375705018005330052400105/125/150270/110313055
VHT 100/..450550450100751900350052500131/155/175290/1403on request85
VHT 250/..6007506002501753000143003100180/210/-2on requeston requeston request
VHT 500/..7509007505003503200145003300220/260/-2on requeston requeston request
1With separated switching system unit 4Depending on furnace design connected load might be higher 21800 °C/2200 °C 5Dimensions may be smaller depending on the heater type 31200 °C/1600 °C
 

Retort furnace VHT 100/15-KE H2 with fiber insulation and extension package for operation under hydrogen, 1400 °C Retort furnace VHT 40/16-MO H2 with hydrogen extension package and process box

Gas management system

H2 Version for Operation with Hydrogen or other Reaction Gases

In the H2 version the retort furnaces can be operated under hydrogen or other reaction gases. For these applications, the systems are additionally equipped with the required safety technology. Only certified and industry proven safety sensors are used. The retort furnaces are controlled by a fail-safe PLC control system (S7-300F/safety controller).

  • Certified safety concept
  • Automation package
  • Redundant gas inlet valves for hydrogen
  • Monitored pre-pressures of all process gases
  • Bypass for safe purging of furnace chamber with inert gas
  • Pressure-monitored emergency flooding with automated solenoid valve opening
  • Electric or gas-heated exhaust gas torch for H2 post-combustion
  • Atmospheric operation: H2-purging of retort starting from room temperature at controlled over pressure (50 mbar relative)

Additional equipment

  • Partial pressure operation: H2 flushing at underpressure in the retort starting from 750  °C furnace chamber temperature
  • Inner process hood in the retort for debinding under hydrogen
  • Process control and documentation via Nabertherm Control Center (NCC) for monitoring, documentation and control
 

Bottom Loading Retort Furnace up to 2400 °C

Retort furnace LBVHT 250/20-W with tungsten heating chamber Retort furnace LBVHT 600/24-GR

Retort furnace LBVHT with graphite heating chamber

The LBVHT model series with bottom loading specification are especially suitable for production processes which require either protective or reaction gase atmosphere or a vacuum. The basic performance specifications of these models are similar to the VHT models. Their size and design with electro-hydraulically driven table facilitate charging during production. The retort furnaces are available in various sizes and designs. Similar like the VHT models, these furnaces can be equipped with different heating concepts.

  • Standard furnace sizes between 100 and 600 liters
  • Designed as bottom loading retort furnace with electro-hydraulically driven table for easy and well-arranged charging
  • Prepared to carry heavy charge weights
  • Different heating concepts using
    • Graphite heating chamber up to Tmax 2400  C
    • Molybdenum heating chamber up to Tmax 1600  C
    • Tungsten heating chamber up to Tmax 2000  C
  • Frame structure filled with textured stainless steel sheets
  • Standard design with gassing system for non-flammable protective or reaction gases
  • Automatic gas supply system which also allows for operation with several process gases as additional equipment
  • Gas supply systems for operating with hydrogen or other combustible reaction gases incl. safety package as additional equipment
  • Switchgear and control box as well as gassing system integrated into the furnace housing
  • Further product characteristics of the standard furnace as well as possible additional equipment can be found in the description of the VHT furnaces
ModelTmaxModelTmaxModelTmaxInner dimensions in mmVolumeElectrical
 °C °C °CØhin lconnection*
LBVHT 100/16-MO1600LBVHT 100/20-W2000LBVHT 100/24-GR24004507001003-phase
LBVHT 250/16-MO1600LBVHT 250/20-W2000LBVHT 250/24-GR24006009002503-phase
LBVHT 600/16-MO1600LBVHT 600/20-W2000LBVHT 600/24-GR240080012006003-phase
*Please see page 89 for more information about supply voltage
 

Cold-Wall Retort Furnaces up to 2400 °C or up to 3000 °C

Retort furnace SVHT 9/24-W with tungsten heating

Graphite heating module

Cylindrical retort with tungsten heating

Cooling water distribution

Compared with the VHT models (page 26 ff), the retort furnaces of the SVHT product line offer improved performance data with regard to achievable vacuum and maximum temperature. Due to the design as pit-type furnace with tungsten heating, processes up to max. 2400 °C even in high vacuum can be implemented with retort furnaces of the SVHT..-W product line. Retort furnaces of the SVHT..-GR product line with graphite heating, also in pit-type design, can be operated in an inert gas atmosphere even up to max. 3000 °C.

  • Standard sizes with a furnace chamber of 2 or 9 liters
  • Designed as pit-type furnace, charged from above
  • Frame construction with inserted sheets of textured stainless steel
  • Dual shell water-cooled stainless steel container
  • Manual operation of process gas and vacuum functions
  • Manual gas supply for non-combustible process gas
  • A step in front of the retort furnace for an ergonomic charging height
  • Retort lid with gas-charged shock absorbers
  • Controls and switchgear as well as gas supply integrated in furnace housing
  • Defined application within the constraints of the operating instructions
  • Further standard product characteristics see description for standard design of VHT models

Heating Options

SVHT ..-GR

  • Applicable for processes:
    • Under protective or reaction gases or in the vacuum up to 2200 C under consideration of relevant max. temperature limits
    • Under inert gas argon up to 3000  C
  • Max. vacuum up to 10-4 mbar depending on the type of pump used
  • Heating: graphite heating elements in cylindrical arrangement
  • Insulation: graphite felt insulation
  • Temperature measurement by means of an optical pyrometer

SVHT ..-W

  • Applicable for processes under protective or reaction gases or in vacuum up to 2400  °C
  • Max. vacuum up to 10-5 mbar depending on the type of pump used
  • Heating: cylindrical tungsten heating module
  • Insulation: tungsten and molybdenum radiant plates
  • Optical temperature measurement with pyrometer
  • Additional equipment such as automatic process gas control or design for the operation with flammable gases incl. safety system see VHT models
ModelTmaxWork space dimensionsUseful volumeOuter dimensions in mmHeating powerElectrical
 °CØ x h in mmin lWDHin KW1connection*
SVHT 2/24-W2400150 x 1502,5130025002000553-phase
SVHT 9/24-W2400230 x 2309,5140029002100953-phase
         
SVHT 2/30-GR3000150 x 1502,5140027502100653-phase
SVHT 9/30-GR3000230 x 2309,5150029002100903-phase
1Depending on furnace design connected load might be higher *Please see page 89 for more information about supply voltage